Crystal structure of bis 4-benzyl piperidinium bis dihydrogenmonophosphate trihydrogenmonophosphate
Language
en
Article de revue
This item was published in
Journal of Chemical Crystallography. 2006, vol. 36, n° 2, p. 111-116
Springer Verlag
English Abstract
The salt bis 4-benzyl piperidinium bis dihydrogenmonophosphate trihydrogenmonophosphate (bis 4-BPP bis DPT) is monoclinic with the following unit cell dimensions: a = 13.132(2) Å, b = 8.755(2) Å, c = 13.643(2) Å, β = 92.40(2)°, ...Read more >
The salt bis 4-benzyl piperidinium bis dihydrogenmonophosphate trihydrogenmonophosphate (bis 4-BPP bis DPT) is monoclinic with the following unit cell dimensions: a = 13.132(2) Å, b = 8.755(2) Å, c = 13.643(2) Å, β = 92.40(2)°, space group P21 with Z = 2. The structure was solved by the Patterson method and refined to final R value of 0.0430. The structure consists of infinite parallel two-dimensional planes built of mutually H2PO4 −, H3PO4 tetrahedra and cations connected by strong O-H···O and N-H···O hydrogen bonding. There are no contacts other than van der Waals interactions between the layers.Read less <
English Keywords
Phosphates
Organic compounds
Crystal structure
Patterson method
X-ray diffraction
Origin
Hal imported