Synthesis and characterization of micro/nanoscale VO2(M) through vanadylethylene glycolate decomposition
Langue
en
Article de revue
Ce document a été publié dans
Inorganic Chemistry. 2021-09-06, vol. 60, n° 17, p. 12709-12713
American Chemical Society
Résumé en anglais
Thanks to a homemade dynamic vacuum system, fully crystallized VO2 (M) is successfully synthesized in a merged step of vanadyl ethylene glycolate (VEG) decomposition and crystallization of VO2 at high temperatures (>500 ...Lire la suite >
Thanks to a homemade dynamic vacuum system, fully crystallized VO2 (M) is successfully synthesized in a merged step of vanadyl ethylene glycolate (VEG) decomposition and crystallization of VO2 at high temperatures (>500 °C). During the whole process, vanadium valence (+4) is well maintained, and VEG microstructure plays an important role in the end-product size and shape. Finally, the suggested route appears well suitable for the mass production of VO2 nanoparticles.< Réduire
Mots clés en anglais
Morphology
Crystallinity
Crystallization
Precursors
Organic reactions
Origine
Importé de halUnités de recherche