Synthesis and characterization of micro/nanoscale VO2(M) through vanadylethylene glycolate decomposition
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en
Article de revue
Este ítem está publicado en
Inorganic Chemistry. 2021-09-06, vol. 60, n° 17, p. 12709-12713
American Chemical Society
Resumen en inglés
Thanks to a homemade dynamic vacuum system, fully crystallized VO2 (M) is successfully synthesized in a merged step of vanadyl ethylene glycolate (VEG) decomposition and crystallization of VO2 at high temperatures (>500 ...Leer más >
Thanks to a homemade dynamic vacuum system, fully crystallized VO2 (M) is successfully synthesized in a merged step of vanadyl ethylene glycolate (VEG) decomposition and crystallization of VO2 at high temperatures (>500 °C). During the whole process, vanadium valence (+4) is well maintained, and VEG microstructure plays an important role in the end-product size and shape. Finally, the suggested route appears well suitable for the mass production of VO2 nanoparticles.< Leer menos
Palabras clave en inglés
Morphology
Crystallinity
Crystallization
Precursors
Organic reactions
Orígen
Importado de HalCentros de investigación