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Optimization of polyphenols extraction from grapevine canes using natural deep eutectic solvents

dc.rights.licenseopenen_US
hal.structure.identifierUnité de Recherche Œnologie [Villenave d'Ornon] [OENO]
dc.contributor.authorPETIT, Eva
hal.structure.identifierUnité de Recherche Œnologie [Villenave d'Ornon] [OENO]
dc.contributor.authorROUGER, Caroline
IDREF: 158011724
hal.structure.identifierUnité de Recherche Œnologie [Villenave d'Ornon] [OENO]
dc.contributor.authorGRIFFAULT, Elie
hal.structure.identifierUnité de Recherche Œnologie [Villenave d'Ornon] [OENO]
dc.contributor.authorFERRER, Anaïs
dc.contributor.authorRENOUF, Elodie
hal.structure.identifierUnité de Recherche Œnologie [Villenave d'Ornon] [OENO]
dc.contributor.authorCLUZET, Stephanie
dc.date.accessioned2024-04-10T09:09:00Z
dc.date.available2024-04-10T09:09:00Z
dc.date.issued2023-09
dc.identifier.urihttps://oskar-bordeaux.fr/handle/20.500.12278/197401
dc.description.abstractEnCanes as vineyard by-products are an underutilized resource for the recovery of polyphenols, as compounds present within these by-products still contribute to biological function that could be of interest for human health. The aim of this paper is to propose an environmentally conscious extraction method aimed towards polyphenols, providing an alternative for conventional organic solvents used. For the first time, we investigated the capacity of natural deep eutectic solvent (NaDES) to recover polyphenols from grapevine canes. Three choline chloride based NaDES systems were investigated in a first step. All were efficient to extract grapevine polyphenols and choline chloride:1,4-butanediol (BCH) provided the best results. Preliminary experiments testing solvent composition, solid to liquid ratio (SLR), temperature and time of extraction determined the experimental domain. A Box-Benhken design with water content (5–27.5–50), solid to liquid ratio (10–30-50 mg/500 µL of BCH), temperature (20–50-80 °C), extraction time (5–32.5–60 min) was applied to improve both polyphenolics levels and antioxidant capacity. Multi-response optimization suggested a SLR ratio of 50 mg/500 µL, a water content of 38.2% (w/w), a temperature of 80 °C and a time of extraction of 17.2 min as optimal extraction parameters. Experimental validation confirmed the predicted results obtained for the extract at optimal conditions. Phytochemical characterization showed that the optimal extract contained high proportions of stilbenes, and more particularly of trans-resveratrol and trans-ε-viniferin. Thus, it was shown that NaDES, as a green alternative to conventional organic solvents, are efficient to extract polyphenols from canes. © 2023, The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.
dc.language.isoENen_US
dc.title.enOptimization of polyphenols extraction from grapevine canes using natural deep eutectic solvents
dc.typeArticle de revueen_US
dc.identifier.doi10.1007/s13399-023-04919-xen_US
dc.subject.halSciences du Vivant [q-bio]/Biologie végétaleen_US
bordeaux.journalBiomass Conversion and Biorefineryen_US
bordeaux.page1161-1197en_US
bordeaux.volume21en_US
bordeaux.hal.laboratoriesOenologie - UMR 1366en_US
bordeaux.issue2en_US
bordeaux.institutionUniversité de Bordeauxen_US
bordeaux.institutionBordeaux INPen_US
bordeaux.institutionINRAEen_US
bordeaux.peerReviewedouien_US
bordeaux.inpressnonen_US
hal.popularnonen_US
hal.audienceInternationaleen_US
hal.exportfalse
dc.rights.ccPas de Licence CCen_US
bordeaux.COinSctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Biomass%20Conversion%20and%20Biorefinery&rft.date=2023-09&rft.volume=21&rft.issue=2&rft.spage=1161-1197&rft.epage=1161-1197&rft.au=PETIT,%20Eva&ROUGER,%20Caroline&GRIFFAULT,%20Elie&FERRER,%20Ana%C3%AFs&RENOUF,%20Elodie&rft.genre=article


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