BENOIT, Roland; WARMONT, Fabienne; MEYNEN, V.; DE WITTE, K.; COOL, P.; TRÉGUER-DELAPIERRE, Mona; SABOUNGI, Marie-Louise

doi:10.1016/j.micromeso.2008.12.017

Metadatos

Mostrar el registro completo del ítem

Licencia de uso del documento

BENOIT, Roland
Centre de Recherche sur la Matière Divisée [CRMD]

WARMONT, Fabienne
Centre de Recherche sur la Matière Divisée [CRMD]

MEYNEN, V.
Laboratory of Adsorption and Catalysis

Idioma

Article de revue

Este ítem está publicado en

Microporous and Mesoporous Materials. 2009, vol. 120, n° 1-2, p. 2-6

Elsevier

Resumen en inglés

Various methods proposed for preparing nanoparticles within porous matrices involve generally the impregnation of the matrix with a solution of precursors followed by reduction based on chemical, thermal, radiolytic, or photochemical process. In most cases, the amount of solution impregnated is small and not uniformly distributed in the matrix, with a yield less than 30% and concentrated around the matrix surface. We have developed a novel method for preparing composite materials, combining impregnation under partial vacuum with radiolytic reduction. This method has enabled us to obtain SBA-15 mesoporous silicas with 50–70% impregnation and to control the nanoparticle size.< Leer menos

Palabras clave en inglés

TEM

Mesoporous silica

Bismuth nanoparticles

Radiolysis

XPS

Metadatos

Licencia de uso del documento

Optimisation of the surface properties of SBA-15 mesoporous silica for in-situ nanoparticle synthesis

Idioma

Este ítem está publicado en

Resumen en inglés

Palabras clave en inglés

DOI

Orígen

Centros de investigación