LIU, Che-Jen; GADELMEIER, Christian; LU, Shao-Lun; YEH, Jien-Wei; YEN, Hung-Wei; GORSSE, Stéphane; GLATZEL, Uwe; YEH, An-Chou

doi:10.1016/j.actamat.2022.118188

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LIU, Che-Jen
High Entropy Materials Center
PhD. Program in Prospective Functional Materials Industry,

GADELMEIER, Christian
Metals and Alloys

LU, Shao-Lun
Department of Materials Science and Engineering
Advanced Application Centre for Microscopy & Microanalysis

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Acta Materialia. 2022, vol. 237, p. 118188

Elsevier

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Tensile creep, which is one of the most important deformation modes for high temperature applications, is rarely reported for refractory high entropy alloys (RHEAs). In the present study, the optical floating zone (OFZ) technique was used to fabricate HfNbTaTiZr with grain size larger than 1 mm on average; tensile creep tests under vacuum at 1100-1250℃ and stepwise loading of 5-30 MPa were conducted. The stress exponents and creep activation energies were determined to be 2.5-2.8 and 273 ± 15 kJ mol-1 , respectively. The stress exponents determined have suggested solute drag creep behavior, and deformation was governed by a/2<111> type dislocations. To elucidate the effect of alloying constituents on solute drag creep, intrinsic diffusion coefficients of all elements were determined by simulation, and theoretical minimum creep strain rates were compared with those of experimental values. Analysis suggests that creep rate of HfNbTaTiZr appears to be controlled by Ta, which possesses the lowest intrinsic diffusivity and contributes the most to drag dislocations. To our knowledge, this work is the first to report tensile creep deformation mechanism of HfNbTaTiZr, especially up to 1250℃.< Réduire

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Refractory high entropy alloy

Creep

High-temperature deformation

Diffusion

Thermally activated processes

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Tensile creep behavior of HfNbTaTiZr refractory high entropy alloy at elevated temperatures

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