Powder bed laser sintering of copper-doped hydroxyapatite: Numerical and experimental parametric analysis
BAZIN, Tiphaine
Institut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
Institut de Recherche sur les CERamiques [IRCER]
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Institut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
Institut de Recherche sur les CERamiques [IRCER]
BAZIN, Tiphaine
Institut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
Institut de Recherche sur les CERamiques [IRCER]
< Réduire
Institut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
Institut de Recherche sur les CERamiques [IRCER]
Langue
en
Article de revue
Ce document a été publié dans
Additive Manufacturing. 2021, vol. 46, p. 102044
Elsevier
Résumé en anglais
Additive manufacturing (AM), especially powder bed laser sintering (PBLS), has been an increasingly popular field since the 1980s. Direct SLS is particularly challenging with ceramic materials due to their low thermal ...Lire la suite >
Additive manufacturing (AM), especially powder bed laser sintering (PBLS), has been an increasingly popular field since the 1980s. Direct SLS is particularly challenging with ceramic materials due to their low thermal conductivity, high melting point, and brittle mechanical behaviour. In addition, they require longer processing times for a reliable sintering degree. In this work, the impact of some crucial parameters in SLS applied to a copper-doped hydroxyapatite bioceramic was studied. Incorporating copper ions into the hydroxyapatite matrix by thermal treatment can stimulate blood vessel formation, simultaneously improving the material's mechanical integrity and antibacterial properties. Moreover, it facilitates laser power absorption by the material at the laser wavelength. Thin films were prepared with controlled thicknesses using dip-coating on glass substrates, and they were irradiated by an ytterbium laser (1.070 µm wavelength). Experimental laser irradiation was systematically compared to numerical models to predict the maximum temperature produced on the film surface by laser irradiation. The evaluated parameters are the absorptivity from the copper concentration, the film thickness, and the laser source (scanning velocity and power). Combining low laser scanning speeds with low film thickness and optimised absorption tuned by the copper concentration has made possible the development of well-sintered ceramics by the PBLS technique.< Réduire
Mots clés en anglais
Powder Bed laser sintering
Hydroxyapatite
Experimental analysis
Numerical model
Copper
Selective laser sintering
Origine
Importé de hal