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Characterization of lithium phosphorus oxide thin film libraries by Laser-Induced Breakdown Spectroscopy imaging: A step towards high-throughput quantitative analyses

hal.structure.identifierCEA Tech Nouvelle-Aquitaine [DNAQ]
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorBERTHOU, William
hal.structure.identifierCEA Tech Nouvelle-Aquitaine [DNAQ]
dc.contributor.authorLEGALLAIS, Maxime
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorBOUSQUET, Bruno
hal.structure.identifierDépartement de l'électricité et de l'hydrogène pour les transports [DEHT]
dc.contributor.authorMOTTO-ROS, V.
hal.structure.identifierDépartement de l'électricité et de l'hydrogène pour les transports [DEHT]
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorLE CRAS, Frédéric
dc.date.issued2024
dc.identifier.issn0584-8547
dc.description.abstractEnElemental analysis is a challenge for the development of High Throughput Experimentation (HTE) on thin film materials, and an even greater one when it comes to screening lithium-containing battery materials. In this regard, Laser-Induced Breakdown Spectroscopy has been evaluated here for the quantitative analysis of lithium in libraries of Li2.3PO3.65 amorphous solid electrolyte films. The LIBS analysis of multiple samples with the same composition, but with thicknesses ranging from 50 to 700 nm, has revealed a linear trend in the intensity ratio of the Li I 610.35 nm and P I 214.91 nm emission lines, opening the way to rapid quantitative analysis of material libraries. The sensitivity of the technique finally allowed the detection of the Li I 670.79 nm emission line for film thicknesses down to 4 nm, corresponding to 0.2% of the ablated volume, or about 0.15 pg of Li
dc.language.isoen
dc.publisherElsevier
dc.title.enCharacterization of lithium phosphorus oxide thin film libraries by Laser-Induced Breakdown Spectroscopy imaging: A step towards high-throughput quantitative analyses
dc.typeArticle de revue
dc.identifier.doi10.1016/j.sab.2024.106906
dc.subject.halChimie/Chimie inorganique
dc.subject.halChimie/Chimie analytique
dc.subject.halChimie/Matériaux
bordeaux.journalSpectrochimica Acta Part B: Atomic Spectroscopy
bordeaux.page106906
bordeaux.volume215
bordeaux.peerReviewedoui
hal.identifiercea-04529021
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//cea-04529021v1
bordeaux.COinSctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Spectrochimica%20Acta%20Part%20B:%20Atomic%20Spectroscopy&rft.date=2024&rft.volume=215&rft.spage=106906&rft.epage=106906&rft.eissn=0584-8547&rft.issn=0584-8547&rft.au=BERTHOU,%20William&LEGALLAIS,%20Maxime&BOUSQUET,%20Bruno&MOTTO-ROS,%20V.&LE%20CRAS,%20Fr%C3%A9d%C3%A9ric&rft.genre=article


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