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Erratum to: Development and application of a multi-residue method for the determination of 53 pharmaceuticals in water, sediment, and suspended solids using liquid chromatography-tandem mass spectrometry

dc.rights.licenseopenen_US
hal.structure.identifierEnvironnements et Paléoenvironnements OCéaniques [EPOC]
dc.contributor.authorAMINOT, Yann
dc.contributor.authorLITRICO, Xavier
dc.contributor.authorCHAMBOLLE, Mélodie
dc.contributor.authorARNAUD, Christine
hal.structure.identifierEnvironnements et Paléoenvironnements OCéaniques [EPOC]
dc.contributor.authorPARDON, Patrick
hal.structure.identifierEnvironnements et Paléoenvironnements OCéaniques [EPOC]
dc.contributor.authorBUDZINSKI, Hélène
ORCID: 0000-0003-1028-9154
IDREF: 070478090
dc.date.accessioned2024-03-28T14:39:58Z
dc.date.available2024-03-28T14:39:58Z
dc.date.issued2015-09-01
dc.identifier.issn1618-2642en_US
dc.identifier.urihttps://www.researchgate.net/publication/281637519_Erratum_to_Development_and_application_of_a_multi-residue_method_for_the_determination_of_53_pharmaceuticals_in_water_sediment_and_suspended_solids_using_liquid_chromatography-tandem_mass_spectrometry
dc.identifier.urioai:crossref.org:10.1007/s00216-015-9095-2
dc.identifier.urioai:researchgate.net:281637519
dc.identifier.urioai:crossref.org:10.1007/s00216-015-9017-3
dc.identifier.urihttps://oskar-bordeaux.fr/handle/20.500.12278/189075
dc.description.abstractEnComprehensive source and fate studies of pharmaceuticals in the environment require analytical methods able to quantify a wide range of molecules over various therapeutic classes, in aqueous and solid matrices. Considering this need, the development of an analytical method to determine 53 pharmaceuticals in aqueous phase and in solid matrices using a combination of microwave-assisted extraction, solid phase extraction, and liquid chromatography coupled with tandem mass spectrometry is reported. Method was successfully validated regarding linearity, repeatability, and overall protocol recovery. Method detection limits (MDLs) do not exceed 1 ng L−1 for 40 molecules in aqueous matrices (6 ng L−1 for the 13 remaining), while subnanogram per gram MDLs were reached for 38 molecules in solid phase (29 ng g−1 for the 15 remaining). Losses due to preparative steps were assessed for the 32 analytes associated to their labeled homologue, revealing an average loss of 40 % during reconcentration, the most altering step. Presence of analytes in wastewater treatment plant (WWTP) effluent aqueous phase and suspended solids (SS) as well as in river water, SS, and sediments was then investigated on a periurban river located in the suburbs of Bordeaux, France, revealing a major contribution of WWTP effluent to the river contamination. Sorption on river SS exceeded 5 % of total concentration for amitriptyline, fluoxetine, imipramine, ritonavir, sildenafil, and propranolol and appeared to be submitted to a seasonal influence. Sediment contamination was lower than the one of SS, organic carbon content, and sediment fine element proportion was accountable for the highest measured concentrations.
dc.language.isoENen_US
dc.sourcecrossref
dc.sourceresearchgate
dc.title.enErratum to: Development and application of a multi-residue method for the determination of 53 pharmaceuticals in water, sediment, and suspended solids using liquid chromatography-tandem mass spectrometry
dc.typeArticle de revueen_US
dc.subject.halSciences de l'environnementen_US
bordeaux.journalAnalytical and Bioanalytical Chemistryen_US
bordeaux.volume407en_US
bordeaux.hal.laboratoriesEPOC : Environnements et Paléoenvironnements Océaniques et Continentaux - UMR 5805en_US
bordeaux.issue28en_US
bordeaux.institutionUniversité de Bordeauxen_US
bordeaux.institutionCNRSen_US
bordeaux.teamLPTCen_US
bordeaux.peerReviewedouien_US
bordeaux.inpressnonen_US
bordeaux.import.sourcedissemin
hal.identifierhal-04525190
hal.version1
hal.date.transferred2024-03-28T14:40:01Z
hal.popularnonen_US
hal.audienceInternationaleen_US
hal.exporttrue
workflow.import.sourcedissemin
dc.rights.ccPas de Licence CCen_US
bordeaux.COinSctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Analytical%20and%20Bioanalytical%20Chemistry&rft.date=2015-09-01&rft.volume=407&rft.issue=28&rft.eissn=1618-2642&rft.issn=1618-2642&rft.au=AMINOT,%20Yann&LITRICO,%20Xavier&CHAMBOLLE,%20M%C3%A9lodie&ARNAUD,%20Christine&PARDON,%20Patrick&rft.genre=article


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