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hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorFAURE, Lauriane
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorMOLINARI, Flora
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorCARFANTAN, Morgane
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorMAGLIONE, Mario
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorJOSSE, Michaël
dc.date.issued2023
dc.identifier.issn0272-8842
dc.description.abstractEnIn this study, Titanium oxyhydroxyide powder was synthetized using a modified sol-gel route. This powder is widely studied as a catalyst for CO2 desorption but is here synthesized for the Cool-SPS sintering of titania based ceramics, as a reactive precursor. It is then important to maximize its reactivity at low temperature. The influence of different synthesis parameters (base used, temperature) on the final properties of the TiO(OH)2 powder is thus investigated. The final products were characterized by XRD, FTIR, SEM, granulometry and TGA. The microstructural parameters are crucial in order to obtain a satisfying reactivity for low temperature sintering and will determine the best parameters for the synthesis of TiO(OH)2. Preliminary results concerning the sintering of TiO2 from this precursor are also reported.
dc.language.isoen
dc.publisherElsevier
dc.subject.enSol-Gel synthesis
dc.subject.enTiO(OH)2
dc.subject.enreactivity
dc.subject.enmicrostructure
dc.subject.enCool-SPS
dc.subject.enAnatase Ceramic
dc.title.enSynthesis of TiO(OH)2 precursor for low temperature sintering: A chemical and microstructural study
dc.typeArticle de revue
dc.identifier.doi10.1016/j.ceramint.2023.06.088
dc.subject.halChimie/Matériaux
bordeaux.journalCeramics International
bordeaux.page28337-28343
bordeaux.volume49
bordeaux.issue17, Part A
bordeaux.peerReviewedoui
hal.identifierhal-04151830
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-04151830v1
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