A Continuous-Flow Polymerization Microprocess with Online GPC and Inline Polymer Recovery by Micromixer-Assisted Nanoprecipitation
| dc.rights.license | open | |
| hal.structure.identifier | Ecole nationale supérieure de chimie, polymères et materiaux de strasbourg (ECPM) | |
| dc.contributor.author | BALLY, Florence | |
| hal.structure.identifier | Ecole nationale supérieure de chimie, polymères et materiaux de strasbourg (ECPM) | |
| dc.contributor.author | SERRA, Christophe A. | |
| hal.structure.identifier | Laboratoire de Chimie des Polymères Organiques [LCPO] | |
| hal.structure.identifier | Team 4 LCPO : Polymer Materials for Electronic, Energy, Information and Communication Technologies | |
| dc.contributor.author | BROCHON, Cyril | |
| hal.structure.identifier | Conception et application de molécules bioactives [CAMB] | |
| dc.contributor.author | ANTON, Nicolas | |
| hal.structure.identifier | Conception et application de molécules bioactives [CAMB] | |
| dc.contributor.author | VANDAMME, Thierry | |
| hal.structure.identifier | Laboratoire de Chimie des Polymères Organiques [LCPO] | |
| hal.structure.identifier | Team 4 LCPO : Polymer Materials for Electronic, Energy, Information and Communication Technologies | |
| dc.contributor.author | HADZIIOANNOU, Georges | |
| dc.date.accessioned | 2020 | |
| dc.date.available | 2020 | |
| dc.date.issued | 2011 | |
| dc.identifier.issn | 1862-832X | |
| dc.identifier.uri | https://oskar-bordeaux.fr/handle/20.500.12278/20433 | |
| dc.description.abstractEn | A microplant, starting from monomers to produce polymer particles, is described and integrates polymerization reaction, polymer analysis and nanoparticle formation in a single continuous-flow microprocess. Original contribution is brought by online polymer analysis and inline polymer nanoprecipitation. Multi-detection GPC of samples taken at the outlet of the microreactor actually enables the characterization of linear and branched polymers by combining a concentration- and a mass-sensitive detection technique. When the steady state of the microreactor is reached, micromixer-assisted nanoprecipitation of the polymer solution follows, leading to a colloidal suspension of nanoparticles with a narrow particle size distribution. Particle sizes, around 100?nm, can be tuned by process parameters. | |
| dc.language.iso | en | |
| dc.publisher | Wiley-VCH Verlag | |
| dc.subject.en | atom transfer radical polymerization (ATRP) | |
| dc.subject.en | continuous flow | |
| dc.subject.en | microprocesses | |
| dc.subject.en | online monitoring | |
| dc.subject.en | polymer nanoparticles | |
| dc.title.en | A Continuous-Flow Polymerization Microprocess with Online GPC and Inline Polymer Recovery by Micromixer-Assisted Nanoprecipitation | |
| dc.type | Article de revue | |
| dc.identifier.doi | 10.1002/mren.201100047 | |
| dc.subject.hal | Chimie/Polymères | |
| bordeaux.journal | Macromolecular Reaction Engineering | |
| bordeaux.page | 542-547 | |
| bordeaux.volume | 5 | |
| bordeaux.hal.laboratories | Laboratoire de Chimie des Polymères Organiques (LCPO) - UMR 5629 | * |
| bordeaux.issue | 11-12 | |
| bordeaux.institution | Bordeaux INP | |
| bordeaux.institution | Université de Bordeaux | |
| bordeaux.peerReviewed | oui | |
| hal.identifier | hal-00817478 | |
| hal.version | 1 | |
| hal.origin.link | https://hal.archives-ouvertes.fr//hal-00817478v1 | |
| bordeaux.COinS | ctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Macromolecular%20Reaction%20Engineering&rft.date=2011&rft.volume=5&rft.issue=11-12&rft.spage=542-547&rft.epage=542-547&rft.eissn=1862-832X&rft.issn=1862-832X&rft.au=BALLY,%20Florence&SERRA,%20Christophe%20A.&BROCHON,%20Cyril&ANTON,%20Nicolas&VANDAMME,%20Thierry&rft.genre=article |
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