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13C, 25Mg, and 43Ca Solid-State NMR for the Purpose of Dolomitic Marbles Provenance Elucidation

hal.structure.identifierArchéosciences Bordeaux
dc.contributor.authorPIANET, Isabelle
hal.structure.identifierINSTITUT CATALÀ D'ARQUEOLOGIA CLÀSSICA [ICAC]
dc.contributor.authorGUTIÉRREZ GARCIA-M, Anna
hal.structure.identifierUniversitat Autònoma de Barcelona = Autonomous University of Barcelona = Universidad Autónoma de Barcelona [UAB]
dc.contributor.authorSAVIN, Marie-Claire
hal.structure.identifierArchéosciences Bordeaux
dc.contributor.authorFREREBEAU, Nicolas
hal.structure.identifierInstitut Michel Eugène Chevreul - FR 2638 [IMEC]
dc.contributor.authorTRÉBOSC, Julien
hal.structure.identifierConditions Extrêmes et Matériaux : Haute Température et Irradiation [CEMHTI]
dc.contributor.authorFLORIAN, Pierre
hal.structure.identifierDepartamento de Ciencias de la Tierra
dc.contributor.authorLAPUENTE MERCADAL, Pilar
dc.date.issued2023
dc.identifier.issn1996-1944
dc.description.abstractEnThe study of the provenance of dolomitic marble artefacts has become relevant since it was discovered that quarries of this marble other than that of Cape-Vathy located on the island of Thasos have been exploited since Antiquity. To improve our knowledge about the provenance of materials and the extent of their dispersion, multiple archaeometric studies were performed in the past including isotope analyses, petrography, cathodoluminescence, and elemental analyses. In the present work, solid-state nuclear magnetic resonance (NMR) spectroscopy has been added to this panel of techniques. NMR allows the characterization of the material at a molecular level by looking at different nuclei: carbon, magnesium, and calcium. Statistical analysis of the data collected on both quarry samples and archaeologic items was also implemented and clearly demonstrates the efficiency of a holistic approach for provenance elucidation. Finally, the first 25Mg NMR tests have shown the potential of this technique to discriminate between dolomitic marbles of different provenance. The results are discussed in terms of their historical meaning and illustrate the exploitation of sources of dolomitic marbles other than the Greek Thasos source.
dc.description.sponsorshipUsing the world in ancient societies : processes and forms of appropriation of space in Long Time - ANR-10-LABX-0052
dc.language.isoen
dc.publisherMDPI
dc.rights.urihttp://creativecommons.org/licenses/by/
dc.subject.enNMR
dc.subject.enMarble
dc.subject.enStable isotope
dc.subject.enElemental analysis
dc.subject.enProvenance studies
dc.title.en13C, 25Mg, and 43Ca Solid-State NMR for the Purpose of Dolomitic Marbles Provenance Elucidation
dc.typeArticle de revue
dc.identifier.doi10.3390/ma16041468
dc.subject.halChimie/Chimie analytique
dc.subject.halChimie/Matériaux
dc.subject.halSciences de l'Homme et Société/Archéologie et Préhistoire
bordeaux.journalMaterials
bordeaux.page1468
bordeaux.volume16
bordeaux.issue4
bordeaux.peerReviewedoui
hal.identifierhal-03980519
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-03980519v1
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