Synthesis of Ti3SiC2 coatings onto SiC monoliths from molten salts
dc.rights.license | open | en_US |
hal.structure.identifier | Laboratoire des Composites Thermostructuraux [LCTS] | |
dc.contributor.author | CHAHHOU, Bilal | |
dc.contributor.author | LABRUGERE-SARROSTE, Chritine | |
dc.contributor.author | IBALOT, Fabienne | |
dc.contributor.author | DANET, J. | |
hal.structure.identifier | Laboratoire des Composites Thermostructuraux [LCTS] | |
dc.contributor.author | ROGER, Jerome | |
dc.date.accessioned | 2023-01-24T14:46:51Z | |
dc.date.available | 2023-01-24T14:46:51Z | |
dc.date.issued | 2022-10 | |
dc.identifier.issn | 0955-2219 | en_US |
dc.identifier.uri | https://oskar-bordeaux.fr/handle/20.500.12278/171770 | |
dc.description.abstractEn | Coatings with composition close to Ti3SiC2 were obtained on SiC substrates from Ti and Si powders with the molten NaCl method. In this work, the growth of coatings by reaction in the salt between monolithic SiC substrates and titanium powder is obtained between 1000 and 1200 °C. At 1000 °C, a coating of 8 µm thickness is formed in 10 h whereas a thin coating of 0.5 µm has been grown in 2 h. A lack in silicon was first found in the coatings prepared at 1100 and 1200 °C. For these temperatures, the addition of silicon powder in the melt had a favorable effect on the final composition, which is found very close to the composition of Ti3SiC2. The reaction mechanism implies the formation of TiCx layers in direct contact with the SiC substrate and the presence of more or less important quantities of Ti3SiC2 and Ti5Si3Cx in the upper layers. | |
dc.language.iso | EN | en_US |
dc.subject.en | Coating | |
dc.subject.en | Molten salt | |
dc.subject.en | Silicon carbide | |
dc.subject.en | Synthesis | |
dc.subject.en | TiSiC | |
dc.title.en | Synthesis of Ti3SiC2 coatings onto SiC monoliths from molten salts | |
dc.title.alternative | Journal of the European Ceramic Society | en_US |
dc.type | Article de revue | en_US |
dc.identifier.doi | 10.1016/j.jeurceramsoc.2022.05.054 | en_US |
dc.subject.hal | Sciences de l'ingénieur [physics]/Matériaux | en_US |
bordeaux.journal | Journal of the European Ceramic Society | en_US |
bordeaux.page | 5484-5492 | en_US |
bordeaux.volume | 42 | en_US |
bordeaux.hal.laboratories | Laboratoire des Composites Thermo Structuraux (LCTS) - UMR 5801 | en_US |
bordeaux.issue | 13 | en_US |
bordeaux.institution | Université de Bordeaux | en_US |
bordeaux.institution | CNRS | en_US |
bordeaux.institution | CEA | en_US |
bordeaux.peerReviewed | oui | en_US |
bordeaux.inpress | non | en_US |
hal.export | false | |
dc.rights.cc | Pas de Licence CC | en_US |
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