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Investigation of the pyrolysis mechanisms of cellobiose in the presence of a polysiloxane

hal.structure.identifierInstitut des Sciences Moléculaires [ISM]
dc.contributor.authorBIROT, Marc
hal.structure.identifierInstitut des Sciences Moléculaires [ISM]
dc.contributor.authorPILLOT, Jean-Paul
hal.structure.identifierUniversité Sciences et Technologies - Bordeaux 1 [UB]
dc.contributor.authorDAUDÉ, Gérard
hal.structure.identifierLaboratoire des Composites Thermostructuraux [LCTS]
dc.contributor.authorPAILLER, René
hal.structure.identifierLaboratoire des Composites Thermostructuraux [LCTS]
dc.contributor.authorGUETTE, Alain
hal.structure.identifierSnecma Propulsion Solide [SPS]
dc.contributor.authorPLAISANTIN, Hervé
hal.structure.identifierSnecma Propulsion Solide [SPS]
dc.contributor.authorLOISON, Sylvie
hal.structure.identifierSnecma Propulsion Solide [SPS]
dc.contributor.authorOLRY, Pierre
hal.structure.identifierCentre de recherches sur les matériaux à haute température [CRMHT]
hal.structure.identifierConditions Extrêmes et Matériaux : Haute Température et Irradiation [CEMHTI]
dc.contributor.authorSIMON, Patrick
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorLABRUGÈRE, Christine
hal.structure.identifierInstitut des Sciences Moléculaires [ISM]
dc.contributor.authorPÉTRAUD, Michel
dc.date.issued2008
dc.identifier.issn0165-2370
dc.description.abstractEnTreatment of cellulose yarns by a polysiloxane followed by a fast pyrolysis step gave carbon fibres exhibiting strong enhancement of their mechanical resistance. To account for the beneficial effect of the polysiloxane, an investigation of the pyrolysis mechanisms was performed on a model system based on cellobiose and a polysiloxane resin. A chemical interaction between cellobiose and the resin (e.g. grafting of siloxane fragments onto the cellobiose) was established by using various physicochemical analysis techniques: nuclear magnetic resonance (NMR), photoelectron spectrometry (XPS), electronic paramagnetic resonance (EPR), Flash pyrolysis–gas chromatography–mass spectrometry (FP/GC/MS) and IR.
dc.language.isoen
dc.publisherElsevier
dc.subject.enCarbon fibre
dc.subject.enCellobiose
dc.subject.enPolysiloxane
dc.subject.enPyrolysis
dc.subject.enRedistributions
dc.title.enInvestigation of the pyrolysis mechanisms of cellobiose in the presence of a polysiloxane
dc.typeArticle de revue
dc.identifier.doi10.1016/j.jaap.2007.12.004
dc.subject.halChimie/Matériaux
bordeaux.journalJournal of Analytical and Applied Pyrolysis
bordeaux.page263-271
bordeaux.volume81
bordeaux.issue2
bordeaux.peerReviewedoui
hal.identifierhal-00258871
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-00258871v1
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