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Impact of synthesis conditions in Na-rich Prussian Blue Analogs

hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
hal.structure.identifierInstitut Charles Gerhardt Montpellier - Institut de Chimie Moléculaire et des Matériaux de Montpellier [ICGM]
hal.structure.identifierRéseau sur le stockage électrochimique de l'énergie [RS2E]
dc.contributor.authorSANZ CAMACHO, Paula
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
hal.structure.identifierInstitut Charles Gerhardt Montpellier - Institut de Chimie Moléculaire et des Matériaux de Montpellier [ICGM]
hal.structure.identifierRéseau sur le stockage électrochimique de l'énergie [RS2E]
dc.contributor.authorWERNERT, Romain
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorDUTTINE, Mathieu
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorWATTIAUX, Alain
hal.structure.identifierDepartment of Mechanical Engineering [Singapore]
hal.structure.identifierDepartment of Material Science and Engineering
dc.contributor.authorRUDOLA, Ashish
hal.structure.identifierDepartment of Mechanical Engineering [Singapore]
dc.contributor.authorBALAYA, Palani
hal.structure.identifierCELLS ALBA synchroton = ALBA Synchrotron [CELLS ALBA]
dc.contributor.authorFAUTH, François
hal.structure.identifierInstitut Charles Gerhardt Montpellier - Institut de Chimie Moléculaire et des Matériaux de Montpellier [ICGM]
hal.structure.identifierRéseau sur le stockage électrochimique de l'énergie [RS2E]
dc.contributor.authorBERTHELOT, Romain
hal.structure.identifierInstitut Charles Gerhardt Montpellier - Institut de Chimie Moléculaire et des Matériaux de Montpellier [ICGM]
hal.structure.identifierRéseau sur le stockage électrochimique de l'énergie [RS2E]
hal.structure.identifierAdvanced Lithium Energy Storage Systems - ALISTORE-ERI [ALISTORE-ERI]
dc.contributor.authorMONCONDUIT, L.
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
hal.structure.identifierRéseau sur le stockage électrochimique de l'énergie [RS2E]
hal.structure.identifierAdvanced Lithium Energy Storage Systems - ALISTORE-ERI [ALISTORE-ERI]
dc.contributor.authorCARLIER, Dany
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
hal.structure.identifierRéseau sur le stockage électrochimique de l'énergie [RS2E]
hal.structure.identifierAdvanced Lithium Energy Storage Systems - ALISTORE-ERI [ALISTORE-ERI]
dc.contributor.authorCROGUENNEC, Laurence
dc.date.issued2021
dc.identifier.issn1944-8244
dc.description.abstractEnSodium rich iron hexacyanoferrates were prepared by coprecipitation, hydrothermal route, and under reflux, with or without dehydration. They were obtained with different structures described in cubic, orthorhombic or rhombohedral symmetry, with variable compositions in sodium, water and cationic vacancies, and with a variety of morphologies. This series of sodium rich Prussian Blue Analogs allowed to address the relationship between synthesis conditions, composition, structure, morphology and electrochemical properties in Na-ion batteries. A new orthorhombic phase with the Na 1.8 Fe 2 (CN) 6 •0.7H 2 O composition synthesized by an hydrothermal route at 140°C is reported for the first time, whereas a phase of Na 2 Fe 2 (CN) 6 •2H 2 O composition obtained under reflux, previously described with a monoclinic structure, shows in fact a rhombohedral structure.
dc.description.sponsorshipLaboratory of excellency for electrochemical energy storage - ANR-10-LABX-0076
dc.language.isoen
dc.publisherWashington, D.C. : American Chemical Society
dc.subject.enNa-ion batteries
dc.subject.enPrussian Blue Analogs
dc.subject.enIron hexacyanoferrates
dc.subject.enhydrothermal synthesis
dc.subject.encoprecipitation synthesis
dc.title.enImpact of synthesis conditions in Na-rich Prussian Blue Analogs
dc.typeArticle de revue
dc.identifier.doi10.1021/acsami.1c09378
dc.subject.halChimie/Matériaux
bordeaux.journalACS Applied Materials & Interfaces
bordeaux.page42682–42692
bordeaux.volume13
bordeaux.issue36
bordeaux.peerReviewedoui
hal.identifierhal-03355266
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-03355266v1
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