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Impact of a fragile precursor on the sintering of tin monoxide

hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorSUBHASIS BHOI, Subhransu
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorDUTTINE, Mathieu
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorCHUNG, U-Chan
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorJOSSE, Michaël
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorSUCHOMEL, Matthew
dc.date.issued2022
dc.identifier.issn0955-2219
dc.description.abstractEnThe thermodynamic stability limits of Sn(II) under ambient conditions imposes constraints on the densification of divalent tin based oxides. In the case of tin monoxide (SnO), a low temperature (≤ 300 °C) electric field assisted processing route (Cool-SPS) affords densification up to 90% of theoretical density. This is demonstrated for both conventional SnO and fragile tin(II) oxyhydroxide [Sn6O4(OH)4] precursor powders. The choice of starting precursor impacts both the optimized processing parameters and the resulting ceramic microstructure. Characterization of phase content and stability has been performed on both the precursor powders and resulting ceramics. Preliminary electrochemical property measurements are presented and their connection to observed microstructure and choice of initial precursor is discussed.
dc.language.isoen
dc.publisherElsevier
dc.subject.enTin Monoxide
dc.subject.enCeramics
dc.subject.enSpark Plasma Sintering
dc.subject.enMetastable Materials
dc.subject.enLow Temperature Densification
dc.title.enImpact of a fragile precursor on the sintering of tin monoxide
dc.typeArticle de revue
dc.identifier.doi10.1016/j.jeurceramsoc.2021.11.042
dc.subject.halChimie/Matériaux
bordeaux.journalJournal of the European Ceramic Society
bordeaux.page1493-1500
bordeaux.volume42
bordeaux.issue4
bordeaux.peerReviewedoui
hal.identifierhal-03364257
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-03364257v1
bordeaux.COinSctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Journal%20of%20the%20European%20Ceramic%20Society&rft.date=2022&rft.volume=42&rft.issue=4&rft.spage=1493-1500&rft.epage=1493-1500&rft.eissn=0955-2219&rft.issn=0955-2219&rft.au=SUBHASIS%20BHOI,%20Subhransu&DUTTINE,%20Mathieu&CHUNG,%20U-Chan&JOSSE,%20Micha%C3%ABl&SUCHOMEL,%20Matthew&rft.genre=article


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