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Development of methods for the preparation of radiopure $^{82}$Se sources for the SuperNEMO neutrinoless double-beta decay experiment
dc.contributor.author | RAKHIMOV, Alimardon V. | |
dc.contributor.author | BARABASH, A.S. | |
dc.contributor.author | BASHARINA-FRESHVILLE, A. | |
dc.contributor.author | BLOT, S. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | BONGRAND, M. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | BOURGEOIS, Ch. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | BRETON, D. | |
dc.contributor.author | BREIER, R. | |
dc.contributor.author | BIRDSALL, E. | |
dc.contributor.author | BRUDANIN, V.B. | |
dc.contributor.author | BUREŠOVA, H. | |
hal.structure.identifier | Centre de Physique des Particules de Marseille [CPPM] | |
dc.contributor.author | BUSTO, J. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | CALVEZ, S. | |
dc.contributor.author | CASCELLA, M. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | CERNA, C. | |
dc.contributor.author | CESAR, J.P. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | CHAUVEAU, E. | |
dc.contributor.author | CHOPRA, A. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | CLAVERIE, G. | |
dc.contributor.author | CAPUA, S.De | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | DELALEE, F. | |
hal.structure.identifier | Laboratoire d'Annecy de Physique des Particules [LAPP] | |
dc.contributor.author | DUCHESNEAU, D. | |
dc.contributor.author | EGOROV, V.G. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | EURIN, G. | |
dc.contributor.author | EVANS, J.J. | |
dc.contributor.author | FAJT, L. | |
dc.contributor.author | FILOSOFOV, D.V. | |
dc.contributor.author | FLACK, R. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | GARRIDO, X. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | GOMEZ, H. | |
hal.structure.identifier | Laboratoire de physique corpusculaire de Caen [LPCC] | |
dc.contributor.author | GUILLON, B. | |
dc.contributor.author | GUZOWSKI, P. | |
dc.contributor.author | HODÁK, R. | |
dc.contributor.author | HOLÝ, K. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | HUBER, A. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | HUGON, C. | |
hal.structure.identifier | Laboratoire d'Annecy de Physique des Particules [LAPP] | |
dc.contributor.author | JEREMIE, A. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | JULLIAN, S. | |
dc.contributor.author | KARAIVANOV, D.V. | |
dc.contributor.author | KAUER, M. | |
dc.contributor.author | KLIMENKO, A.A. | |
dc.contributor.author | KOCHETOV, O.I. | |
dc.contributor.author | KONOVALOV, S.I. | |
dc.contributor.author | KOVALENKO, V. | |
dc.contributor.author | LANG, K. | |
hal.structure.identifier | Laboratoire de physique corpusculaire de Caen [LPCC] | |
dc.contributor.author | LEMIÈRE, Y. | |
hal.structure.identifier | Laboratoire d'Annecy de Physique des Particules [LAPP] | |
dc.contributor.author | NOBLET, T.Le | |
dc.contributor.author | LIPTAK, Z. | |
dc.contributor.author | LIU, X.R. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | LOAIZA, P. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | LUTTER, G. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | MAALMI, J. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | MACKO, M. | |
dc.contributor.author | MAMEDOV, F. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | MARQUET, C. | |
hal.structure.identifier | Laboratoire de physique corpusculaire de Caen [LPCC] | |
dc.contributor.author | MAUGER, F. | |
hal.structure.identifier | Laboratoire d'Annecy de Physique des Particules [LAPP] | |
dc.contributor.author | MINOTTI, A. | |
dc.contributor.author | MIRSAGATOVA, A.A. | |
dc.contributor.author | MIRZAYEV, N.A. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | MOREAU, I. | |
dc.contributor.author | MORGAN, B. | |
dc.contributor.author | MOTT, J. | |
dc.contributor.author | NEMCHENOK, I.B. | |
dc.contributor.author | NOMACHI, M. | |
dc.contributor.author | NOVA, F. | |
dc.contributor.author | OHSUMI, H. | |
hal.structure.identifier | Laboratoire de physique corpusculaire de Caen [LPCC] | |
dc.contributor.author | OLIVIERO, G. | |
dc.contributor.author | PAHLKA, R.B. | |
dc.contributor.author | PATER, J.R. | |
dc.contributor.author | PALUŠOVÁ, V. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | PERROT, F. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | PIQUEMAL, F. | |
dc.contributor.author | POVINEC, P. | |
dc.contributor.author | PRIDAL, P. | |
dc.contributor.author | RAMACHERS, Y.A. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | REBII, A. | |
hal.structure.identifier | Laboratoire d'Annecy de Physique des Particules [LAPP] | |
dc.contributor.author | REMOTO, A. | |
dc.contributor.author | RICHARDS, B. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | RICOL, J.S. | |
dc.contributor.author | RUKHADZE, E. | |
dc.contributor.author | RUKHADZE, N.I. | |
dc.contributor.author | SAAKYAN, R. | |
dc.contributor.author | SADIKOV, I.I. | |
dc.contributor.author | SALAZAR, R. | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | SARAZIN, X. | |
dc.contributor.author | SEDGBEER, J. | |
dc.contributor.author | SHITOV, Yu. A. | |
dc.contributor.author | ŠIMKOVIC, F. | |
hal.structure.identifier | Institut universitaire de France [IUF] | |
hal.structure.identifier | Laboratoire de l'Accélérateur Linéaire [LAL] | |
dc.contributor.author | SIMARD, L. | |
dc.contributor.author | SMETANA, A. | |
dc.contributor.author | SMOLEK, K. | |
dc.contributor.author | SMOLNIKOV, A.A. | |
dc.contributor.author | SNOW, S. | |
dc.contributor.author | SÖLDNER-REMBOLD, S. | |
hal.structure.identifier | Centre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG] | |
dc.contributor.author | SOULÉ, B. | |
dc.contributor.author | ŠPAVOROVA, M. | |
dc.contributor.author | ŠTEKL, I. | |
dc.contributor.author | TASHIMOVA, F.A. | |
dc.contributor.author | THOMAS, J. | |
dc.contributor.author | TIMKIN, V. | |
dc.contributor.author | TORRE, S. | |
dc.contributor.author | TRETYAK, Vl. I. | |
dc.contributor.author | TRETYAK, V.I. | |
dc.contributor.author | UMATOV, V.I. | |
dc.contributor.author | VILELA, C. | |
dc.contributor.author | VOROBEL, V. | |
hal.structure.identifier | Laboratoire de Physique Subatomique et de Cosmologie [LPSC] | |
dc.contributor.author | WAROT, G. | |
dc.contributor.author | WATERS, D. | |
hal.structure.identifier | Laboratoire de Physique Subatomique et de Cosmologie [LPSC] | |
dc.contributor.author | ZAMPAOLO, M. | |
dc.contributor.author | ŽUKAUSKAS, A. | |
dc.date.issued | 2020 | |
dc.description.abstractEn | <jats:title>Abstract</jats:title><jats:p>A radiochemical method for producing <jats:sup>82</jats:sup>Se sources with an ultra-low level of contamination of natural radionuclides (<jats:sup>40</jats:sup>K, decay products of <jats:sup>232</jats:sup>Th and <jats:sup>238</jats:sup>U) has been developed based on cation-exchange chromatographic purification with reverse removal of impurities. It includes chromatographic separation (purification), reduction, conditioning (which includes decantation, centrifugation, washing, grinding, and drying), and <jats:sup>82</jats:sup>Se foil production. The conditioning stage, during which highly dispersed elemental selenium is obtained by the reduction of purified selenious acid (H<jats:sub>2</jats:sub>SeO<jats:sub>3</jats:sub>) with sulfur dioxide (SO<jats:sub>2</jats:sub>) represents the crucial step in the preparation of radiopure <jats:sup>82</jats:sup>Se samples. The natural selenium (600 g) was first produced in this procedure in order to refine the method. The technique developed was then used to produce 2.5 kg of radiopure enriched selenium (<jats:sup>82</jats:sup>Se). The produced <jats:sup>82</jats:sup>Se samples were wrapped in polyethylene (12 μm thick) and radionuclides present in the sample were analyzed with the BiPo-3 detector. The radiopurity of the plastic materials (chromatographic column material and polypropylene chemical vessels), which were used at all stages, was determined by instrumental neutron activation analysis. The radiopurity of the <jats:sup>82</jats:sup>Se foils was checked by measurements with the BiPo-3 spectrometer, which confirmed the high purity of the final product. The measured contamination level for <jats:sup>208</jats:sup>Tl was 8–54 μBq/kg, and for <jats:sup>214</jats:sup>Bi the detection limit of 600 μBq/kg has been reached.</jats:p> | |
dc.language.iso | en | |
dc.subject.en | Selenium-82 | |
dc.subject.en | ion exchange chromatography | |
dc.subject.en | purification | |
dc.subject.en | mass spectrometry | |
dc.subject.en | neutron activation analysis | |
dc.subject.en | SuperNEMO | |
dc.subject.en | LSM Modane | |
dc.subject.en | double-beta decay: (0neutrino) | |
dc.subject.en | ion: exchange | |
dc.subject.en | selenium: nuclide | |
dc.subject.en | selenium: production | |
dc.subject.en | background: radioactivity | |
dc.subject.en | Neutrino Ettore Majorana Observatory | |
dc.subject.en | sulfur | |
dc.subject.en | oxygen | |
dc.subject.en | chemistry | |
dc.subject.en | fabrication | |
dc.subject.en | measurement methods | |
dc.title.en | Development of methods for the preparation of radiopure $^{82}$Se sources for the SuperNEMO neutrinoless double-beta decay experiment | |
dc.type | Article de revue | |
dc.identifier.doi | 10.1515/ract-2019-3129 | |
dc.subject.hal | Physique [physics] | |
bordeaux.journal | Radiochim.Acta | |
bordeaux.page | 87-97 | |
bordeaux.volume | 108 | |
bordeaux.issue | 2 | |
bordeaux.peerReviewed | oui | |
hal.identifier | hal-02491286 | |
hal.version | 1 | |
hal.popular | non | |
hal.audience | Internationale | |
hal.origin.link | https://hal.archives-ouvertes.fr//hal-02491286v1 | |
bordeaux.COinS | ctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Radiochim.Acta&rft.date=2020&rft.volume=108&rft.issue=2&rft.spage=87-97&rft.epage=87-97&rft.au=RAKHIMOV,%20Alimardon%20V.&BARABASH,%20A.S.&BASHARINA-FRESHVILLE,%20A.&BLOT,%20S.&BONGRAND,%20M.&rft.genre=article |
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