Synthesis, Crystal Structure and Characterization of [(CH3CH2)4N]Mn1,5Cl34H2OCl2(H2O)
| dc.contributor.author | DHOUIB, Ikram | |
| hal.structure.identifier | Institut de Chimie de la Matière Condensée de Bordeaux [ICMCB] | |
| dc.contributor.author | GUIONNEAU, Philippe | |
| dc.contributor.author | MHIRI, Tahar | |
| dc.contributor.author | ELAOUD, Zakaria | |
| dc.date.issued | 2014 | |
| dc.identifier.issn | 2321-807X | |
| dc.description.abstractEn | Single crystals of [(CH3CH2)4N] Mn1,5 Cl3 4H2O Cl 2(H2O) were grown by the slow evaporation technique and characterized by means of single-crystal X-ray diffraction, FT-IR and Raman spectroscopy. The title compound belongs to the triclinic space group P with the following unit cell dimensions: a =7.5425(4) Å, b=9.8464 Å, c=13.7671(6) Å, α=89.951(3)°,β=89.753(3)°, γ=81.861(3)°, Z=4. These structures have solved using direct methods and refined by least-squares analysis. The structure was solved by the direct method and refined to final R value of 0.0567. The projection of [(CH3CH2)4N] Mn1,5 Cl3 4H2O Cl 2(H2O) in the plan (a,b) shows an arrangement in layers perpendicular to the direction b . The structure consists of infinite parallel two-dimensional planes built connected ions and water molecules by strong O-H...O and O-H...Cl hydrogen bonding. | |
| dc.language.iso | en | |
| dc.publisher | Khalsa Publications | |
| dc.subject.en | Hybrid compound | |
| dc.subject.en | X-ray diffraction | |
| dc.subject.en | Infrared spectroscopy | |
| dc.subject.en | Raman spectroscopy | |
| dc.title.en | Synthesis, Crystal Structure and Characterization of [(CH3CH2)4N]Mn1,5Cl34H2OCl2(H2O) | |
| dc.type | Article de revue | |
| dc.identifier.doi | 10.24297/jac.v8i2.4044 | |
| dc.subject.hal | Chimie/Matériaux | |
| dc.subject.hal | Chimie/Cristallographie | |
| bordeaux.journal | Journal of Advances in Chemistry | |
| bordeaux.page | 1639-1650 | |
| bordeaux.volume | 8 | |
| bordeaux.issue | 2 | |
| bordeaux.peerReviewed | oui | |
| hal.identifier | hal-00988825 | |
| hal.version | 1 | |
| hal.popular | non | |
| hal.audience | Internationale | |
| hal.origin.link | https://hal.archives-ouvertes.fr//hal-00988825v1 | |
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