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hal.structure.identifierCentre de recherches Paul Pascal [CRPP]
dc.contributor.authorRECULUSA, Stéphane
hal.structure.identifierCentre de recherches Paul Pascal [CRPP]
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorPONCET-LEGRAND, Céline
hal.structure.identifierCentre de recherches Paul Pascal [CRPP]
dc.contributor.authorRAVAINE, Serge
hal.structure.identifierInteractions moléculaires et réactivité chimique et photochimique [IMRCP]
dc.contributor.authorMINGOTAUD, Christophe
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorDUGUET, Etienne
hal.structure.identifierLaboratoire de chimie et procédés de polymérisation [LCPP]
dc.contributor.authorBOURGEAT-LAMI, Elodie
dc.date.issued2002
dc.identifier.issn0897-4756
dc.description.abstractEnRaspberrylike hybrid organic−inorganic materials consisting of spherical silica beads supporting smaller polystyrene particles were prepared through a heterophase polymerization process. In a first step, micrometer-sized silica particles were synthesized according to procedures inspired from the literature. In a second step, a poly(ethylene glycol) macromonomer was adsorbed on the surface of the silica beads. Finally, polymerization of styrene was achieved in water with a nonionic surfactant as an emulsifying agent and sodium persulfate as an initiator. Scanning and transmission electron microscopies show that the presence of the macromonomer on the surface of the silica particles is a determining parameter in order to get the raspberrylike morphology.
dc.language.isoen
dc.publisherAmerican Chemical Society
dc.subject.enPolymerization
dc.subject.enHybrid materials
dc.subject.enSilica
dc.subject.enPolystyrene
dc.title.enSyntheses of raspberrylike silica/polystyrene materials
dc.typeArticle de revue
dc.identifier.doi10.1021/cm0116525
dc.subject.halChimie/Matériaux
bordeaux.journalChemistry of Materials
bordeaux.page2354-2359
bordeaux.volume14
bordeaux.issue5
bordeaux.peerReviewedoui
hal.identifierhal-00715951
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-00715951v1
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