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Lithium conducting solid electrolyte Li1.3Al0.3Ti1.7(PO4)3 obtained via solution chemistry

hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorDULUARD, Sandrine
hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorPAILLASSA, Aude
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorPUECH, Laurent
hal.structure.identifierInstitut de Chimie de la Matière Condensée de Bordeaux [ICMCB]
dc.contributor.authorVINATIER, Philippe
hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorTURQ, Viviane
hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorROZIER, Patrick
hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorLENORMAND, Pascal
hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorTABERNA, P.-L.
hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorSIMON, Patrice
hal.structure.identifierCentre interuniversitaire de recherche et d'ingénierie des matériaux [CIRIMAT]
dc.contributor.authorANSART, Florence
dc.date.issued2013
dc.identifier.issn0955-2219
dc.description.abstractEnNaSICON-type lithium conductor Li1.3Al0.3Ti1.7(PO4)3 (LATP) is synthesized with controlled grain size and composition using solution chemistry. After thermal treatment at 850 °C, sub-micronic crystallized powders with high purity are obtained. They are converted into ceramic through Spark Plasma Sintering at 850-1000 °C. By varying the processing parameters, pellet with conductivities up to 1.6 × 10−4 S/cm with density of 97% of the theoretical density have been obtained. XRD, FEG-SEM, ac-impedance and Vickers indentation were used to characterize the products. The influence of sintering parameters on pellet composition, microstructure and conductivity is discussed in addition to the analysis of the mechanical behavior of the grains interfaces.
dc.language.isoen
dc.publisherElsevier
dc.subject.enPowders-chemical preparation
dc.subject.enSintering
dc.subject.enMicrostructure
dc.subject.enIonic conductivity
dc.subject.enBatteries
dc.title.enLithium conducting solid electrolyte Li1.3Al0.3Ti1.7(PO4)3 obtained via solution chemistry
dc.typeArticle de revue
dc.identifier.doi10.1016/j.jeurceramsoc.2012.08.005
dc.subject.halChimie/Matériaux
bordeaux.journalJournal of the European Ceramic Society
bordeaux.page1145-1153
bordeaux.volume33
bordeaux.issue6
bordeaux.peerReviewedoui
hal.identifierhal-00793078
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-00793078v1
bordeaux.COinSctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Journal%20of%20the%20European%20Ceramic%20Society&rft.date=2013&rft.volume=33&rft.issue=6&rft.spage=1145-1153&rft.epage=1145-1153&rft.eissn=0955-2219&rft.issn=0955-2219&rft.au=DULUARD,%20Sandrine&PAILLASSA,%20Aude&PUECH,%20Laurent&VINATIER,%20Philippe&TURQ,%20Viviane&rft.genre=article


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