JANČAŘÍK, Andrej; HOLEC, Jan; NAGATA, Yuuya; ŠÁMAL, Michal; GOURDON, Andre

doi:10.1038/s41467-021-27809-0

JANČAŘÍK, Andrej
Centre de Recherche Paul Pascal [CRPP]

HOLEC, Jan

NAGATA, Yuuya

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Nature Communications. 2022-01, vol. 13, n° 1

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AbstractDuring the last years we have witnessed progressive evolution of preparation of acenes with length up to dodecacene by on-surface synthesis in ultra-high vacuum or generation of acenes up to decacene in solid matrices at low temperatures. While these protocols with very specific conditions produce the acenes in amount of few molecules, the strategies leading to the acenes in large quantities dawdle behind. Only recently and after 70 years of synthetic attempts, heptacene has been prepared in bulk phase. However, the preparative scale synthesis of higher homologues still remains a formidable challenge. Here we report the preparation and characterisation of nonacene and show its excellent thermal and in-time stability.< Leer menos

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https://oskar-bordeaux.fr/handle/20.500.12278/140250

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http://dx.doi.org/10.1038/s41467-021-27809-0

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https://static-content.springer.com/esm/art%3A10.1038%2Fs41467-021-27809-0/MediaObjects/41467_2021_27809_MOESM1_ESM.pdf

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Centre de Recherche Paul Pascal (CRPP) - UMR 5031

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Preparative-scale synthesis of nonacene

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