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A new thermo-desorption laser-heating setup for studying noble gas diffusion and release from materials at high temperatures

hal.structure.identifierCentre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG]
dc.contributor.authorHORLAIT, Denis
hal.structure.identifierCentre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG]
dc.contributor.authorFAURE, Rémi
hal.structure.identifierCentre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG]
dc.contributor.authorTHOMAS, Bertrand
hal.structure.identifierCentre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG]
dc.contributor.authorDEVERT, Nicolas
hal.structure.identifierConditions Extrêmes et Matériaux : Haute Température et Irradiation [CEMHTI]
dc.contributor.authorAMANY, Marie-Lyne
hal.structure.identifierDépartement d'Etudes des Combustibles [DEC]
dc.contributor.authorCARLOT, Gaëlle
hal.structure.identifierCentre d'Etudes Nucléaires de Bordeaux Gradignan [CENBG]
dc.contributor.authorGILABERT, Éric
dc.date.issued2021
dc.identifier.issn0034-6748
dc.description.abstractEnA new heating and gas treatment line for Thermo-Desorption Spectrometry (TDS) of noble gases (He, Ne, Ar, Kr and Xe) is presented. It was built with the primary objective to offer advanced temperature controls and capabilities while working in a cold-environment. By choosing a high-power continuous wave laser as an heating source, and using a Proportional-Integral-Derivative (PID) controller system, noble gases TDS can now be performed with fast and highly steady heating ramps (e.g. less than 1°C deviation from setpoint for ≤ 1°C.s-1 ramps). Sample temperature over 2000°C can also routinely be reached, with limited heating of the sample support and the sample chamber, offering the possibility to have several samples awaiting in the ultra-high vacuum chamber. We also present development efforts made to increase temperature homogeneity of the heated sample while limiting contacts with the sample holder. Recent results acquired with this TDS setup on krypton thermal diffusion in uranium dioxide (UO 2) as a function of O 2 additions are also presented as an application example.
dc.language.isoen
dc.publisherAmerican Institute of Physics
dc.subject.enThermo-Desorption Spectroscopy
dc.subject.enNoble Gases
dc.subject.enLaser Heating
dc.subject.enNuclear Materials
dc.title.enA new thermo-desorption laser-heating setup for studying noble gas diffusion and release from materials at high temperatures
dc.typeArticle de revue
dc.identifier.doi10.1063/5.0068858
dc.subject.halPhysique [physics]/Physique [physics]/Instrumentations et Détecteurs [physics.ins-det]
dc.subject.halSciences de l'ingénieur [physics]/Matériaux
bordeaux.journalReview of Scientific Instruments
bordeaux.page124102
bordeaux.volume92
bordeaux.issue12
bordeaux.peerReviewedoui
hal.identifierhal-03465516
hal.version1
hal.popularnon
hal.audienceInternationale
hal.origin.linkhttps://hal.archives-ouvertes.fr//hal-03465516v1
bordeaux.COinSctx_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.jtitle=Review%20of%20Scientific%20Instruments&rft.date=2021&rft.volume=92&rft.issue=12&rft.spage=124102&rft.epage=124102&rft.eissn=0034-6748&rft.issn=0034-6748&rft.au=HORLAIT,%20Denis&FAURE,%20R%C3%A9mi&THOMAS,%20Bertrand&DEVERT,%20Nicolas&AMANY,%20Marie-Lyne&rft.genre=article


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